5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt

Base Information

Chemical Name:5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt
CAS No.:1350629-68-3
Molecular Formula:C₆H₁₅N*C₃₃H₃₂N₆O₂
Molecular Weight:645.848
Hs Code.:

Synonyms:5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt

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Chemical Property of 5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt

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Technology Process of 5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt

There total 4 articles about 5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 791644-32-1
methyl 3,5-bis[bis(pyridin-2-ylmethyl)aminomethyl]benzoate

: 1350629-68-3
5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt

Guidance literature:: methyl 3,5-bis[bis(pyridin-2-ylmethyl)aminomethyl]benzoate; With sodium hydroxide; In methanol; for 2h; Resolution of racemate;

With triethylamine;

Reference yield: 95.0%

: 791644-32-1
methyl 3,5-bis[bis(pyridin-2-ylmethyl)aminomethyl]benzoate

: 121-44-8
triethylamine

: 1350629-68-3
5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt

Guidance literature:: methyl 3,5-bis[bis(pyridin-2-ylmethyl)aminomethyl]benzoate; With water; sodium hydroxide; In methanol; for 2h; Reflux;

triethylamine; In water;
DOI:10.1039/c1ob06154b

Reference yield:

: 25081-39-4
methyl 3,5-dimethylbenzoate

: 1350629-68-3
5-bis[[bis(2-pyridylmethyl)amino]methyl]benzoic acid triethylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux

1.2: 0 - 20 °C

2.1: potassium carbonate / acetonitrile / 70 °C

3.1: water; sodium hydroxide / methanol / 2 h / Reflux

With N-Bromosuccinimide; water; potassium carbonate; sodium hydroxide; dibenzoyl peroxide; In methanol; tetrachloromethane; acetonitrile;
DOI:10.1039/c1ob06154b