(R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

Base Information

Chemical Name:(R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone
CAS No.:403656-69-9
Molecular Formula:C₃₈H₃₉NO₇
Molecular Weight:621.73
Hs Code.:

Synonyms:(R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

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Technology Process of (R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

There total 1 articles about (R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 90110-63-7
3-methoxybenzyl iodide

: 403656-65-5
(4R)-4-(diphenylmethyl)-3-[(3R)-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

: 403656-69-9
(R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -54 ℃; for 26h;
DOI:10.1021/jo015501x

Reference yield: 88.0%

: 403656-69-9
(R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

: 403656-70-2
(2R,3R)-2,3-bis-(3'-methoxybenzyl)succininc acid 4-ethyl ester

Guidance literature:: (R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone; With lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 0.0333333h;

With dihydrogen peroxide; In tetrahydrofuran; water; at 0 ℃; for 3h; Further stages.;
DOI:10.1021/jo015501x

Reference yield:

: 403656-69-9
(R)-4-(diphenylmethyl)-3-[(2R,3R)-2-(3'-methoxyphenyl)methyl-3-(ethoxycarbonyl)-4-(3'-methoxyphenyl)]butanoyl-2-oxazolidinone

: 80704-91-2
(3R,4R)-3,4-bis<(3-methoxyphenyl)methyl>dihydro-2(3H)-furanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: LiOH*H₂O / tetrahydrofuran; H₂O / 0.03 h / 0 °C

1.2: 88 percent / H₂O₂ / tetrahydrofuran; H₂O / 3 h / 0 °C

2.1: LiBH₄; MeOH / diethyl ether / 24 h / 20 °C

3.1: 126 mg / p-toluenesulfonic acid / benzene / 4 h / Heating

With methanol; lithium hydroxide; lithium borohydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; water; benzene;
DOI:10.1021/jo015501x