adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide

Base Information

Chemical Name:adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide
CAS No.:318499-37-5
Molecular Formula:C₁₉H₂₅N₃O₂
Molecular Weight:327.426
Hs Code.:

Synonyms:adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide

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Chemical Property of adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide

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Technology Process of adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide

There total 4 articles about adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 318499-27-3
2-adamantan-1-yl-6-methyl-benzo[d][1,3]oxazin-4-one

: 318499-37-5
adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide

Guidance literature:: With hydrazine hydrate; at 80 ℃; for 3h;
DOI:10.1002/1521-4184(200010)333:10<323::AID-ARDP323>3.0.CO;2-U

Reference yield:

: 2941-78-8
2-Amino-5-methylbenzoic acid

: 318499-37-5
adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / NEt₃ / CH₂Cl₂ / 10 h / 20 °C

2: 55 percent / Ac₂O / 4 h / Heating

3: 58 percent / N₂H₄*H₂O / 3 h / 80 °C

With acetic anhydride; hydrazine hydrate; triethylamine; In dichloromethane;
DOI:10.1002/1521-4184(200010)333:10<323::AID-ARDP323>3.0.CO;2-U

Reference yield:

: 2094-72-6
1-Adamantanecarbonyl chloride

: 318499-37-5
adamantane-1-carboxylic acid (2-hydrazinocarbonyl-4-methyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / NEt₃ / CH₂Cl₂ / 10 h / 20 °C

2: 55 percent / Ac₂O / 4 h / Heating

3: 58 percent / N₂H₄*H₂O / 3 h / 80 °C

With acetic anhydride; hydrazine hydrate; triethylamine; In dichloromethane;
DOI:10.1002/1521-4184(200010)333:10<323::AID-ARDP323>3.0.CO;2-U