C₂₉H₄₆N₂O₇

Base Information

Chemical Name:C₂₉H₄₆N₂O₇
CAS No.:1034401-95-0
Molecular Formula:C₂₉H₄₆N₂O₇
Molecular Weight:534.693
Hs Code.:

C<sub>29</sub>H<sub>46</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₉H₄₆N₂O₇

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Chemical Property of C₂₉H₄₆N₂O₇

Chemical Property:

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Technology Process of C₂₉H₄₆N₂O₇

There total 12 articles about C₂₉H₄₆N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1034401-93-8
C₂₃H₃₅NO₆

: 6456-74-2
Glycine tert-butyl ester

: 1034401-95-0
C₂₉H₄₆N₂O₇

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2008.03.107

Reference yield:

: (2R,3R,4S,5S)-6-(4-Methoxy-benzyloxy)-3,5-dimethyl-hexane-1,2,4-triol

: 1034401-95-0
C₂₉H₄₆N₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium periodate / tetrahydrofuran; water / 2 h / 0 - 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: 0.5 h / 0 °C

3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 760.05 Torr

4.1: 1H-imidazole / tetrahydrofuran / 8 h / 0 °C

5.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 5 h / 0 - 20 °C

6.1: camphor-10-sulfonic acid / methanol; dichloromethane / 0.5 h / 0 °C

7.1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

8.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate dihydrate / water; tert-butyl alcohol / 1 h / 20 °C

9.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0.17 h / 0 °C

9.2: 0 °C

With 1H-imidazole; dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; palladium 10% on activated carbon; camphor-10-sulfonic acid; hydrogen; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; 2.1: |Wittig Olefination / 2.2: |Wittig Olefination / 7.1: |Parikh-Doering Oxidation;
DOI:10.1016/j.tetasy.2013.07.012

Reference yield:

: C₂₀H₃₂O₃

: 1034401-95-0
C₂₉H₄₆N₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 760.05 Torr

2.1: 1H-imidazole / tetrahydrofuran / 8 h / 0 °C

3.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 5 h / 0 - 20 °C

4.1: camphor-10-sulfonic acid / methanol; dichloromethane / 0.5 h / 0 °C

5.1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

6.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate dihydrate / water; tert-butyl alcohol / 1 h / 20 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0.17 h / 0 °C

7.2: 0 °C

With 1H-imidazole; dmap; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; palladium 10% on activated carbon; camphor-10-sulfonic acid; hydrogen; sulfur trioxide pyridine complex; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; 5.1: |Parikh-Doering Oxidation;
DOI:10.1016/j.tetasy.2013.07.012