5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

Base Information

Chemical Name:5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione
CAS No.:125758-77-2
Molecular Formula:C₂₄H₃₁NO₄SSi
Molecular Weight:457.666
Hs Code.:

Synonyms:5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

Suppliers and Price of 5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

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Chemical Property of 5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

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Technology Process of 5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

There total 8 articles about 5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141221-12-7
5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>phenylmethylene>thiazolidine-2,4-dione

: 125758-77-2
5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

Guidance literature:: With sodium amalgam; In methanol; for 20h; Yield given;
DOI:10.1021/jm00088a022

Reference yield:

: 36372-16-4
1-(4-bromophenyl)-2-phenoxyethan-1-one

: 125758-77-2
5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: sodium borohydride / propan-2-ol; CH₂Cl₂ / 1 h

2: 61 percent / imidazole / dimethylformamide / 36 h / Ambient temperature

3: 1.) BuLi / 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, DMF, -78 deg C, 1 h

4: sodium acetate / 2 h / 140 °C

5: 3percent sodium amalgam / methanol / 20 h

With 1H-imidazole; sodium tetrahydroborate; sodium amalgam; n-butyllithium; sodium acetate; In methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm00088a022

Reference yield:

: 125734-57-8
1-(4-bromophenyl)-2-phenoxyethan-1-ol

: 125758-77-2
5-<4-<1-<(tert-butyldimethylsilyl)oxy>-2-phenoxyethyl>benzyl>thiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / imidazole / dimethylformamide / 36 h / Ambient temperature

2: 1.) BuLi / 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, DMF, -78 deg C, 1 h

3: sodium acetate / 2 h / 140 °C

4: 3percent sodium amalgam / methanol / 20 h

With 1H-imidazole; sodium amalgam; n-butyllithium; sodium acetate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00088a022