3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol

Base Information

Chemical Name:3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol
CAS No.:90763-11-4
Molecular Formula:C₁₀H₁₂Br₂O₅
Molecular Weight:372.01
Hs Code.:

Synonyms:3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol

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Technology Process of 3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol

There total 2 articles about 3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.5%

: 78138-31-5
3,4-di-O-acetyl-2,6-dibromo-2,6-dideoxy-α-D-glucopyranosyl bromide

: 90762-88-2
Benzyl 3-O-Benzyl-2,6-dideoxy-α-D-arabino-hexopyranoside

: 90763-11-4
3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol

: 90763-06-7
Benzyl 4-O-(3,4-Di-O-acetyl-2,6-dibromo-2,6-dideoxy-β-D-glucopyranosyl)-3-O-benzyl-2,6-dideoxy-α-D-arabino-hexopyranoside

: 90763-05-6
Benzyl 4-O-(3,4-Di-O-acetyl-2,6-dibromo-2,6-dideoxy-α-D-glucopyranosyl)-3-O-benzyl-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: With 2,3,5-trimethyl-pyridine; silver trifluoromethanesulfonate; In nitromethane; dichloromethane; toluene; 1) 6h, -20 to -10 deg 4) roomtemp.;
DOI:10.1021/jo00191a006

Reference yield: 33.0%

: 78138-31-5
3,4-di-O-acetyl-2,6-dibromo-2,6-dideoxy-α-D-glucopyranosyl bromide

: 100-51-6,185532-71-2
benzyl alcohol

: 90763-11-4
3,4-di-O-acetyl-1,5-anhydro-2,6-dibromo-2,6-dideoxy-D-arabino-hex-1-enitol

: 78138-27-9,78184-99-3,135684-09-2
1,3,4-tri-O-acetyl-2,6-dibromo-2,6-dideoxy-α-D-glucopyranose

: 92611-20-6
benzyl 3,4-di-O-acetyl-2,6-dibromo-2,6-dideoxy-β-D-glucopyranoside

: 92611-21-7
benzyl 3,4-di-O-acetyl-2,6-dibromo-2,6-dideoxy-α-D-glucopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at -70 ℃;
DOI:10.1016/0008-6215(84)85275-1