Technology Process of C37H40N2O9
There total 5 articles about C37H40N2O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride; acetic acid;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere
2: ammonium fluoride / methanol / 3 h / 20 °C
3: dmap; triethylamine / acetonitrile / 1 h / 0 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.5 h / 20 °C
With
dmap; ammonium fluoride; tetrabutyl ammonium fluoride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere
3: ammonium fluoride / methanol / 3 h / 20 °C
4: dmap; triethylamine / acetonitrile / 1 h / 0 °C / Inert atmosphere
5: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.5 h / 20 °C
With
2,6-dimethylpyridine; dmap; ammonium fluoride; tetrabutyl ammonium fluoride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
