methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate

Base Information

• Chemical Name: methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate
• CAS No.: 115264-53-4
• Molecular Formula: C₂₆H₂₃NO₃
• Molecular Weight: 397.474

Synonyms:methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate

Chemical Property of methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate

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Technology Process of methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate

There total 1 articles about methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

triphenylketeneimine (14181-84-1) + sodium trichloroacetate (650-51-1) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → N-(2,2-diphenylvinyl)-N-phenylamide dichloroacetic acid (115264-62-5) + N-(2,2-diphenylvinyl)-N-(trichlorovinyl)aniline (115264-63-6) + methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate (115264-53-4) + methyl 2--2-methylpropionate (115264-54-5)

Guidance literature:

N-benzyl-N,N,N-triethylammonium chloride; In chloroform; at 60 ℃; for 4.5h;

DOI:10.1007/BF00476534

Reference yield: 99.0%

methyl 5-benzhydryliden-3-methyl-2-oxo-1-phenylpyrrolidine-3-carboxylate (115264-53-4) → 2-benzhydryliden-4-(hydroxymethyl)-4-methyl-1-phenylpyrrolidine (115264-55-6)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; for 1h; Heating;

DOI:10.1007/BF00476534

upstream raw materials:

triphenylketeneimine

sodium trichloroacetate

methacrylic acid methyl ester

Downstream raw materials:

2-benzhydryliden-4-(hydroxymethyl)-4-methyl-1-phenylpyrrolidine

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