C₃₃H₄₇NO₆Si₂

Base Information

Chemical Name:C₃₃H₄₇NO₆Si₂
CAS No.:1315455-10-7
Molecular Formula:C₃₃H₄₇NO₆Si₂
Molecular Weight:609.91
Hs Code.:

C<sub>33</sub>H<sub>47</sub>NO<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₃H₄₇NO₆Si₂

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Chemical Property of C₃₃H₄₇NO₆Si₂

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Technology Process of C₃₃H₄₇NO₆Si₂

There total 9 articles about C₃₃H₄₇NO₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1315455-09-4
C₃₅H₄₉NO₇Si₂

: 1315455-10-7
C₃₃H₄₇NO₆Si₂

Guidance literature:: With methanol; barium(II) hydroxide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: 1021493-52-6
C₉H₆F₃NO₇S

: 1315455-10-7
C₃₃H₄₇NO₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / methanol / 1.25 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane / 19.5 h / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 27.5 h / 80 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / tetrahydrofuran; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

4.2: 4 h / 20 °C

5.1: pyridinium p-toluenesulfonate / water; benzene / 0.17 h / 20 °C / Inert atmosphere

5.2: 0.17 h / 20 °C / Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

7.1: methanol; barium(II) hydroxide / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; methanol; sodium tetrahydroborate; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; barium(II) hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/chem.201003489

Reference yield:

: 1315455-04-9
C₉H₈F₃NO₇S

: 1315455-10-7
C₃₃H₄₇NO₆Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / dichloromethane / 19.5 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 27.5 h / 80 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

3.2: 4 h / 20 °C

4.1: pyridinium p-toluenesulfonate / water; benzene / 0.17 h / 20 °C / Inert atmosphere

4.2: 0.17 h / 20 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

6.1: methanol; barium(II) hydroxide / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; methanol; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; barium(II) hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/chem.201003489