BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

Base Information

Chemical Name:BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl
CAS No.:77374-84-6
Molecular Formula:C₃₇H₄₆N₆O₆S₃
Molecular Weight:767.007
Hs Code.:

BzlS-CH<sub>2</sub>CH<sub>2</sub>CO-Gly<sub>2</sub>-Cys(Bzl)-Gly<sub>2</sub>-NHCH<sub>2</sub>CH<sub>2</sub>-SBzl

Synonyms:BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

Suppliers and Price of BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

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Technology Process of BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

There total 6 articles about BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 77374-83-5
BzlS-CH₂CH₂CO-Gly₂-ONSu

: 77374-82-4
H-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl*HBr

: 77374-84-6
BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 24h;
DOI:10.1039/P19810000310

Reference yield:

: 50833-62-0
p-nitrophenyl 3-benzylthiopropionate

: 77374-84-6
BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / NaHCO₃ / dimethylformamide; ethanol; H₂O / 24 h

2: 90 percent / N,N'-dicyclohexylcarbodi-imide / ethyl acetate / 1.) 0 deg C, 1-2 h, 2.) room temperature, overnight

3: 92 percent / Et₃N / dimethylformamide / 24 h

With sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/P19810000310

Reference yield:

: 22572-33-4
S-benzylcysteamine hydrochloride

: 77374-84-6
BzlS-CH₂CH₂CO-Gly₂-Cys(Bzl)-Gly₂-NHCH₂CH₂-SBzl

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N / dimethylformamide / 24 h

2: 73 percent / 22.5percent hydrogen bromide / acetic acid / 0.67 h / Ambient temperature

3: 92 percent / Et₃N / dimethylformamide / 24 h

With hydrogen bromide; triethylamine; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/P19810000310