C₂₃H₃₂N₂O₉

Base Information

Chemical Name:C₂₃H₃₂N₂O₉
CAS No.:1407508-18-2
Molecular Formula:C₂₃H₃₂N₂O₉
Molecular Weight:480.515
Hs Code.:

C<sub>23</sub>H<sub>32</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₂₃H₃₂N₂O₉

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Chemical Property of C₂₃H₃₂N₂O₉

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Technology Process of C₂₃H₃₂N₂O₉

There total 8 articles about C₂₃H₃₂N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1407508-17-1
C₂₃H₃₄N₂O₈

: 1407508-18-2
C₂₃H₃₂N₂O₉

Guidance literature:: C₂₃H₃₄N₂O₈; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In dichloromethane; water; at 20 ℃; for 3h;

With hydrogenchloride; In dichloromethane; water; pH=3;
DOI:10.1016/j.tetasy.2012.08.008

Reference yield:

: 241811-68-7
(2S,3S,5R,6R)-3-tert-butyldimethylsilyloxymethyl-2-hydroxymethyl-5,6-dimethoxy-5,6-dimethyl-1,4-dioxane

: 1407508-18-2
C₂₃H₃₂N₂O₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: dmap; pyridine / 0 - 20 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 18 h / 70 °C / Inert atmosphere

3.1: hydrogen; 10% Pd/C / ethyl acetate; ethanol / 3 h / 2585.81 Torr

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 3 h / 20 °C

6.2: pH 3

With pyridine; dmap; sodium azide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; 10% Pd/C; tetrabutyl ammonium fluoride; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2012.08.008

Reference yield:

: 1407508-13-7
(2S,3S,5R,6R)-3-(tert-butyldimethylsilyloxymethyl)-2-(p-toluenesulfonyloxymethyl)-5,6-dimethoxy-5,6-dimethyl-1,4-dioxane

: 1407508-18-2
C₂₃H₃₂N₂O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide / N,N-dimethyl-formamide / 18 h / 70 °C / Inert atmosphere

2.1: hydrogen; 10% Pd/C / ethyl acetate; ethanol / 3 h / 2585.81 Torr

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 3 h / 20 °C

5.2: pH 3

With sodium azide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; 10% Pd/C; tetrabutyl ammonium fluoride; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2012.08.008