3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate

Base Information

Chemical Name:3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate
CAS No.:1448674-55-2
Molecular Formula:C₁₈H₂₇N₃O₆
Molecular Weight:381.429
Hs Code.:

Synonyms:3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate

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Chemical Property of 3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate

Chemical Property:

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Technology Process of 3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate

There total 6 articles about 3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448674-54-1
4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)oxy]butyl acetate

: 1448674-55-2
3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate

Guidance literature:: With hydrazine hydrate; In ethanol; at 20 ℃; for 16h; Cooling;

Reference yield:

: 3,4-dihydroxybutyl acetate

: 1448674-55-2
3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; triethylamine / dichloromethane / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3 h / 0 - 20 °C

3: pyridine hydrogenfluoride / tetrahydrofuran / 16 h / 20 °C

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 0 - 20 °C

5: hydrazine hydrate / ethanol / 16 h / 20 °C / Cooling

With dmap; di-isopropyl azodicarboxylate; pyridine hydrogenfluoride; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 1448674-51-8
4-{[tert-butyl(dimethyl)silyl]oxy}-3-hydroxybutyl acetate

: 1448674-55-2
3-(aminooxy)-4-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}butyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3 h / 0 - 20 °C

2: pyridine hydrogenfluoride / tetrahydrofuran / 16 h / 20 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 0 - 20 °C

4: hydrazine hydrate / ethanol / 16 h / 20 °C / Cooling

With di-isopropyl azodicarboxylate; pyridine hydrogenfluoride; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; ethanol;