(1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol

Base Information

• Chemical Name: (1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol
• CAS No.: 215026-14-5
• Molecular Formula: C₂₀H₂₂O₂
• Molecular Weight: 294.393
• Mol file: 215026-14-5.mol

Synonyms:(1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol

Chemical Property of (1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol

There total 3 articles about (1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H28O3Se → (1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol (215026-14-5)

Guidance literature:

With sodium hydrogencarbonate; In methanol; water; at 90 ℃; for 48h; Yield given;

DOI:10.1039/a804072i

Reference yield:

(S,S)-hydrobenzoin (2325-10-2) → (1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol (215026-14-5)

Guidance literature:

Multi-step reaction with 3 steps

1: BF₃*OEt₂ / 2 h / Ambient temperature

2: NaIO₄, NaHCO₃ / methanol; H₂O / 0.17 h / Ambient temperature

3: NaHCO₃ / methanol; H₂O / 48 h / 90 °C

With sodium periodate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; In methanol; water;

DOI:10.1039/a804072i

Reference yield:

(1S,2S)-1,2-Diphenyl-2-((1S,2S)-2-phenylselanyl-cyclohexyloxy)-ethanol → (1S,2S,1'S)-2-(cyclohex-2'-enyloxy)-1,2-diphenylethanol (215026-14-5)

Guidance literature:

Multi-step reaction with 2 steps

1: NaIO₄, NaHCO₃ / methanol; H₂O / 0.17 h / Ambient temperature

2: NaHCO₃ / methanol; H₂O / 48 h / 90 °C

With sodium periodate; sodium hydrogencarbonate; In methanol; water;

DOI:10.1039/a804072i

upstream raw materials:

(S,S)-hydrobenzoin

Downstream raw materials:

(1S,3S,4S,6S,7S)-3,4-diphenyl-7-phenylseleno-2,5-dioxabicyclo[4,4,0]decane

(1S,2S,3S)-3[(1S,2S)-2-hydroxy-1,2-diphenylethoxy]-1,2-cyclohexanediol

[1S-(1α,3β)]-cyclohexane-1,2,3-triol

D-chiro-inositol