C₃₄H₄₇O₄SiN

Base Information

• Chemical Name: C₃₄H₄₇O₄SiN
• CAS No.: 922493-42-3
• Molecular Formula: C₃₄H₄₇NO₄Si
• Molecular Weight: 561.837
• Mol file: 922493-42-3.mol

Synonyms:C₃₄H₄₇O₄SiN

Chemical Property of C₃₄H₄₇O₄SiN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₄₇O₄SiN

There total 5 articles about C₃₄H₄₇O₄SiN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H37O2SiN3 (922493-41-2) → C34H47O4SiN (922493-42-3)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethyl acetate

2: 2.66 g / triethylamine / CH₂Cl₂ / 20 °C

With hydrogen; triethylamine; platinum(IV) oxide; In dichloromethane; ethyl acetate;

DOI:10.1002/anie.200602033

Reference yield:

(3S,4R)-1-Benzyloxy-4-methyl-hex-5-en-3-ol (909803-71-0) → C34H47O4SiN (922493-42-3)

Guidance literature:

Multi-step reaction with 8 steps

1.1: 1.07 g / pyridine / CH₂Cl₂

2.1: O₃; O₂ / CH₂Cl₂ / -78 °C

2.2: triphenylphosphine / CH₂Cl₂ / 20 °C

3.1: NaBH₄ / ethanol / 0.5 h

3.2: 382 mg / K₂CO₃ / methanol / 24 h / 20 °C

4.1: 90 percent / pyridine; 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 20 °C

5.1: triethylamine / tetrahydrofuran / 20 °C

6.1: 1.96 g / NaN₃ / dimethylformamide / 5 h / 60 °C

7.1: H₂ / PtO₂ / ethyl acetate

8.1: 2.66 g / triethylamine / CH₂Cl₂ / 20 °C

With pyridine; dmap; sodium tetrahydroborate; sodium azide; hydrogen; oxygen; ozone; triethylamine; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1002/anie.200602033

Reference yield:

C15H20O4 → C34H47O4SiN (922493-42-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: NaBH₄ / ethanol / 0.5 h

1.2: 382 mg / K₂CO₃ / methanol / 24 h / 20 °C

2.1: 90 percent / pyridine; 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 20 °C

3.1: triethylamine / tetrahydrofuran / 20 °C

4.1: 1.96 g / NaN₃ / dimethylformamide / 5 h / 60 °C

5.1: H₂ / PtO₂ / ethyl acetate

6.1: 2.66 g / triethylamine / CH₂Cl₂ / 20 °C

With pyridine; dmap; sodium tetrahydroborate; sodium azide; hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1002/anie.200602033

upstream raw materials:

di-tert-butyl dicarbonate

(3S,4R)-1-Benzyloxy-4-methyl-hex-5-en-3-ol

C₂₉H₃₇O₂SiN₃

(2R,3S)-5-Benzyloxy-2-methyl-pentane-1,3-diol

Downstream raw materials:

C₂₇H₄₁O₄SiN

(3R,4S)-3-[(tert-butyloxycarbonyl)amino]-5-[(tert-butyldiphenylsilyl)oxy]-4-methylpentanal

C₃₃H₄₉NO₅Si

C₃₁H₄₅NO₅Si