methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside

Base Information

Chemical Name:methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside
CAS No.:131175-42-3
Molecular Formula:C₂₂H₂₅NO₅
Molecular Weight:383.444
Hs Code.:

Synonyms:methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside

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Chemical Property of methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside

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Technology Process of methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside

There total 1 articles about methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 131053-25-3,131102-05-1
methyl 3-O-benzyl-2,6-imino-2,5,6-trideoxy-D-lyxo-hexofuranoside

: 501-53-1,94274-21-2
benzyl chloroformate

: 131175-42-3
methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside

: 98260-66-3
methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-α-D-lyxo-hexofuranoside

Guidance literature:: With sodium hydrogencarbonate; In diethyl ether; for 18h;
DOI:10.1016/S0957-4166(00)86337-5

Reference yield: 87.0%

: 131175-42-3
methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside

: 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-D-lyxo-hexose

Guidance literature:: With trifluoroacetic acid; for 0.333333h; Ambient temperature;
DOI:10.1016/S0957-4166(00)86337-5

Reference yield:

: 131175-42-3
methyl 3-O-benzyl-N-benzyloxycarbonyl-2,6-imino-2,5,6-trideoxy-β-D-lyxo-hexofuranoside

: 53185-12-9,475630-67-2,637771-88-1
D-fagomine

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / aq. TFA / 0.33 h / Ambient temperature

2: 97 percent / NaBH₄ / ethanol; H₂O / 0.33 h

3: H₂, HOAc / Pd black / 18 h / 760 Torr

With sodium tetrahydroborate; hydrogen; acetic acid; trifluoroacetic acid; palladium; In ethanol; water;
DOI:10.1016/S0957-4166(00)86337-5