3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate

Base Information

Chemical Name:3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate
CAS No.:104856-93-1
Molecular Formula:C₁₂H₁₀Cl₂N₈
Molecular Weight:337.171
Hs Code.:

Synonyms:3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate

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Chemical Property of 3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate

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Technology Process of 3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate

There total 3 articles about 3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 104856-92-0
7-amino-N-(3,4-dichlorophenyl)-5-<(phenylmethyl)thio>pyrimido<5,4-e>-1,2,4-triazine-3-methanamine

: 104856-93-1
3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate

Guidance literature:: With ammonia; In N,N-dimethyl acetamide; at 60 ℃; for 7h;
DOI:10.1002/jhet.5570220547

Reference yield:

: 28363-22-6
<(3,4-dichlorophenyl)amino>acetonitrile

: 104856-93-1
3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate

Guidance literature:: Multi-step reaction with 3 steps

1: Ambient temperature

2: ethanol; dioxane / 24 h / Ambient temperature

3: 77 percent / ethanolic ammonia / N,N-dimethyl-acetamide / 7 h / 60 °C

With ammonia; In 1,4-dioxane; ethanol; N,N-dimethyl acetamide;
DOI:10.1002/jhet.5570220547

Reference yield:

: 104856-91-9
2-<(3,4-dichlorophenyl)amino>ethanimidic acid, ethyl ester

: 104856-93-1
3-<<(3,4-dichlorophenyl)amino>methyl>pyrimido<5,4-e>-1,2,4-triazine-5,7-diamine, hydrate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; dioxane / 24 h / Ambient temperature

2: 77 percent / ethanolic ammonia / N,N-dimethyl-acetamide / 7 h / 60 °C

With ammonia; In 1,4-dioxane; ethanol; N,N-dimethyl acetamide;
DOI:10.1002/jhet.5570220547