C₃₁H₄₁ClO₇Si

Base Information

Chemical Name:C₃₁H₄₁ClO₇Si
CAS No.:1332271-65-4
Molecular Formula:C₃₁H₄₁ClO₇Si
Molecular Weight:589.201
Hs Code.:

C<sub>31</sub>H<sub>41</sub>ClO<sub>7</sub>Si

Synonyms:C₃₁H₄₁ClO₇Si

Suppliers and Price of C₃₁H₄₁ClO₇Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₁H₄₁ClO₇Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₁H₄₁ClO₇Si

There total 8 articles about C₃₁H₄₁ClO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₃₉ClO₇Si

: 1332271-65-4
C₃₁H₄₁ClO₇Si

Guidance literature:: C₃₁H₃₉ClO₇Si; With sodium tetrahydroborate; cerium(III) chloride heptahydrate; In methanol; at 0 ℃; for 0.5h; Inert atmosphere;

With ammonium chloride; In methanol; water; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1332271-27-8
C₃₂H₄₀ClF₃O₁₀SSi

: 1332271-65-4
C₃₁H₄₁ClO₇Si

: 1332271-28-9
C₃₁H₄₁ClO₇Si

Guidance literature:: With chromium dichloride; nickel dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 1h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: C₃₁H₄₅ClO₇Si

: 1332271-65-4
C₃₁H₄₁ClO₇Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 40 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1.17 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

4.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 4 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: chromium dichloride; nickel dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

7.1: pyridine; Dess-Martin periodane / dichloromethane / 4.5 h / 20 °C / Inert atmosphere

8.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.5 h / 0 °C / Inert atmosphere

8.2: Inert atmosphere

With pyridine; chromium dichloride; sodium tetrahydroborate; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; sulfur trioxide pyridine complex; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; Dess-Martin periodane; pyridine hydrogenfluoride; dimethyl sulfoxide; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; 6.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1016/j.tet.2011.04.094