1,3-Cyclopentanediol, 5-(hydroxymethyl)-1-methyl-, (1R,3R,5R)- (9CI)

Base Information

Chemical Name:1,3-Cyclopentanediol, 5-(hydroxymethyl)-1-methyl-, (1R,3R,5R)- (9CI)
CAS No.:524011-38-9
Molecular Formula:C7H14O3
Molecular Weight:146.18426
Hs Code.:
Mol file:524011-38-9.mol

Synonyms:1,3-Cyclopentanediol, 5-(hydroxymethyl)-1-methyl-, (1R,3R,5R)- (9CI)

Suppliers and Price of 1,3-Cyclopentanediol, 5-(hydroxymethyl)-1-methyl-, (1R,3R,5R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 1,3-Cyclopentanediol, 5-(hydroxymethyl)-1-methyl-, (1R,3R,5R)- (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-Cyclopentanediol, 5-(hydroxymethyl)-1-methyl-, (1R,3R,5R)- (9CI)

There total 6 articles about 1,3-Cyclopentanediol, 5-(hydroxymethyl)-1-methyl-, (1R,3R,5R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 524011-37-8
(1S,2S,4R,5R)-4-hydroxy-1-methyl-6-oxa-bicyclo[3.1.0]hexane-2-carboxylic acid ethyl ester

: 524011-38-9
(1R,3R,5R)-5-(hydroxymethyl)-1-methylcyclopentane-1,3-diol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 23h; Heating;
DOI:10.1002/1099-0690(200301)2003:1<92::AID-EJOC92>3.0.CO;2-V

Reference yield: 93.0%

: 524011-35-6
(1S,2R,4R,5R)-2-benzyloxy-4-(benzyloxymethyl)-6-oxabicyclo[3.1.0]hexane

: 524011-38-9
(1S,3R,5R)-5-(hydroxymethyl)-1-methylcyclopentane-1,3-diol

Guidance literature:: (1S,2R,4R,5R)-2-benzyloxy-4-(benzyloxymethyl)-6-oxabicyclo[3.1.0]hexane; With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; for 96h; Heating;

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 24h;
DOI:10.1002/1099-0690(200301)2003:1<92::AID-EJOC92>3.0.CO;2-V

Reference yield:

: 524011-27-6
ethyl (1S,4R)-4-hydroxy-2-methyl-cyclopent-2-ene-1-carboxylate

: 524011-38-9
(1R,3R,5R)-5-(hydroxymethyl)-1-methylcyclopentane-1,3-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / t-BuOOH / VO(acac)2 / benzene / 20 h / Heating

2: 98 percent / LiAlH₄ / diethyl ether / 23 h / Heating

With tert.-butylhydroperoxide; lithium aluminium tetrahydride; bis(acetylacetonate)oxovanadium; In diethyl ether; benzene;
DOI:10.1002/1099-0690(200301)2003:1<92::AID-EJOC92>3.0.CO;2-V