3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol

Base Information

Chemical Name:3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol
CAS No.:719272-69-2
Molecular Formula:C₂₃H₃₃N₃O₂
Molecular Weight:383.534
Hs Code.:

Synonyms:3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol

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Chemical Property of 3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol

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Technology Process of 3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol

There total 9 articles about 3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 719273-35-5
3-[4-(benzyloxy)-2-methoxyphenyl]-4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazole

: 719272-69-2
3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 19h; under 760.051 Torr;

Reference yield:

: 719274-37-0
4-Benzyloxy-2-methoxy-benzonitrile

: 719272-69-2
3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide; triethylamine hydrochloride / toluene / 48 h / 110 °C

2: toluene / 9 h / 120 °C / Heating / reflux

3: potassium carbonate / dichloromethane; water

4: hydrogen / palladium 10% on activated carbon / methanol / 19 h / 20 °C / 760.05 Torr

With sodium azide; hydrogen; triethylamine hydrochloride; potassium carbonate; palladium 10% on activated carbon; In methanol; dichloromethane; water; toluene;

Reference yield:

: 3-[4-(benzyloxy)-2-methoxyphenyl]-4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazole hydrochloride

: 719272-69-2
3-Methoxy-4-[4-methyl-5-(4-pentylbicyclo[2.2.2]oct-1-yl)-4H-1,2,4-triazol-3-yl]phenol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dichloromethane; water

2: hydrogen / palladium 10% on activated carbon / methanol / 19 h / 20 °C / 760.05 Torr

With hydrogen; potassium carbonate; palladium 10% on activated carbon; In methanol; dichloromethane; water;