benzyl 5-[(aminocarbonyl)amino]-6-methyl-4-oxo-5-azaspiro[2.4]hept-6-ene-7-carboxylate

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Chemical Name:benzyl 5-[(aminocarbonyl)amino]-6-methyl-4-oxo-5-azaspiro[2.4]hept-6-ene-7-carboxylate
CAS No.:1177445-82-7
Molecular Formula:C₁₆H₁₇N₃O₄
Molecular Weight:315.329
Hs Code.:

Synonyms:benzyl 5-[(aminocarbonyl)amino]-6-methyl-4-oxo-5-azaspiro[2.4]hept-6-ene-7-carboxylate

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Chemical Property of benzyl 5-[(aminocarbonyl)amino]-6-methyl-4-oxo-5-azaspiro[2.4]hept-6-ene-7-carboxylate

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Technology Process of benzyl 5-[(aminocarbonyl)amino]-6-methyl-4-oxo-5-azaspiro[2.4]hept-6-ene-7-carboxylate

There total 1 articles about benzyl 5-[(aminocarbonyl)amino]-6-methyl-4-oxo-5-azaspiro[2.4]hept-6-ene-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 17082-61-0
1,2-bis(trimethylsiloxy)cyclobutene

: C₁₂H₁₃N₃O₃

: 1177445-82-7
benzyl 5-[(aminocarbonyl)amino]-6-methyl-4-oxo-5-azaspiro[2.4]hept-6-ene-7-carboxylate

Guidance literature:: 1,2-bis(trimethylsiloxy)cyclobutene; C₁₂H₁₃N₃O₃; With bismuth(lll) trifluoromethanesulfonate; In dichloromethane; at 20 ℃; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.04.018