2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Base Information

Chemical Name:2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone
CAS No.:832096-82-9
Molecular Formula:C₆₀H₆₆N₂O₆
Molecular Weight:911.194
Hs Code.:

2-(5-{4-[bis-(4-<i>tert</i>-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[<i>lmn</i>][3,8]phenanthroline-1,3,6,8-tetraone

Synonyms:2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Chemical Property of 2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Technology Process of 2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

There total 4 articles about 2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-[5-(tetrahydro-pyran-2-yloxy)-pentyl]-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

: 832096-82-9
2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane; at 20 ℃; for 4h;
DOI:10.1002/chem.200400651

Reference yield:

: 5259-98-3
5-chloropentan-1-ol

: 832096-82-9
2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / K₂CO₃; LiBr; [18]crown-6 / acetonitrile / 144 h / Heating

2: DEAD; PPh₃ / tetrahydrofuran / 16 h / 20 °C

3: 0.63 g / aq. HCl / methanol; CH₂Cl₂ / 4 h / 20 °C

With hydrogenchloride; 18-crown-6 ether; potassium carbonate; triphenylphosphine; lithium bromide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 2: Mitsunobu reaction;
DOI:10.1002/chem.200400651

Reference yield:

: 177609-50-6
4-[bis[4-(tert-butyl)phenyl][4-(isopropyl)phenyl]methyl]phenol

: 832096-82-9
2-(5-{4-[bis-(4-tert-butyl-phenyl)-(4-isopropyl-phenyl)-methyl]-phenoxy}-pentyl)-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / K₂CO₃; LiBr; [18]crown-6 / acetonitrile / 144 h / Heating

2: DEAD; PPh₃ / tetrahydrofuran / 16 h / 20 °C

3: 0.63 g / aq. HCl / methanol; CH₂Cl₂ / 4 h / 20 °C

With hydrogenchloride; 18-crown-6 ether; potassium carbonate; triphenylphosphine; lithium bromide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 2: Mitsunobu reaction;
DOI:10.1002/chem.200400651