(3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol

Base Information

Chemical Name:(3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol
CAS No.:130662-50-9
Molecular Formula:C₉H₁₁BrO₃
Molecular Weight:247.089
Hs Code.:

Synonyms:(3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol

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Chemical Property of (3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol

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Technology Process of (3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol

There total 5 articles about (3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 130662-49-6
Acetic acid 2-acetoxymethyl-3-bromo-6-methoxy-benzyl ester

: 130662-50-9
(3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol

Guidance literature:: With potassium carbonate; In methanol; water; for 4h; Ambient temperature;

Reference yield:

: 2944-49-2
2,3-dimethylanisole

: 130662-50-9
(3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / N-bromosuccinimide (NBS) / CCl₄ / 1 h / Ambient temperature

2: 100 percent / N-bromosuccinimide (NBS) / CCl₄ / Heating; Irradiation

3: 95 percent / sodium acetate, glacial acetic acid / 3 h / Heating

4: 96 percent / potassium carbonate / methanol; H₂O / 4 h / Ambient temperature

With N-Bromosuccinimide; sodium acetate; potassium carbonate; acetic acid; In methanol; tetrachloromethane; water;

Reference yield:

: 526-75-0
2,3-Dimethylphenol

: 130662-50-9
(3-Bromo-2-hydroxymethyl-6-methoxy-phenyl)-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / tetra-N-butylammonium hydrogensulfate, aq. potassium hydroxide / CH₂Cl₂ / 2 h / Ambient temperature

2: 100 percent / N-bromosuccinimide (NBS) / CCl₄ / 1 h / Ambient temperature

3: 100 percent / N-bromosuccinimide (NBS) / CCl₄ / Heating; Irradiation

4: 95 percent / sodium acetate, glacial acetic acid / 3 h / Heating

5: 96 percent / potassium carbonate / methanol; H₂O / 4 h / Ambient temperature

With potassium hydroxide; N-Bromosuccinimide; sodium acetate; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; acetic acid; In methanol; tetrachloromethane; dichloromethane; water;