cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

Base Information

Chemical Name:cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate
CAS No.:1443999-17-4
Molecular Formula:C₁₆H₂₁NO₃
Molecular Weight:275.348
Hs Code.:

Synonyms:cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

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Technology Process of cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

There total 6 articles about cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1443999-16-3
trans-(4-hydroxy-4-methylcyclohexyl)methyl benzoate

: 77287-34-4,77287-35-5,60100-09-6
formamide

: 1443999-17-4
cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

: 1443999-18-5
trans-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

Guidance literature:: With methanesulfonic acid; trifluoroacetic acid; at 90 ℃; for 8h; Overall yield = 76 %;
DOI:10.1055/s-0032-1318477

Reference yield:

: 1629637-03-1
(4-methylenecyclohexyl)methyl benzoate

: 77287-34-4,77287-35-5,60100-09-6
formamide

: 1443999-17-4
cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

: 1443999-18-5
trans-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

Guidance literature:: With methanesulfonic acid; trifluoroacetic acid; at 90 ℃; for 8h; Reagent/catalyst; Overall yield = 71 %; stereoselective reaction;
DOI:10.1055/s-0033-1338605

Reference yield:

: 1629637-04-2
(4-methylcyclohex-3-en-1-yl)methyl benzoate

: 77287-34-4,77287-35-5,60100-09-6
formamide

: 1443999-17-4
cis-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

: 1443999-18-5
trans-[4-(formylamino)-4-methylcyclohexyl]methyl benzoate

Guidance literature:: With methanesulfonic acid; trifluoroacetic acid; at 90 ℃; for 8h; Overall yield = 71 %; stereoselective reaction;
DOI:10.1055/s-0033-1338605