(E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

Base Information

Chemical Name:(E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol
CAS No.:116103-37-8
Molecular Formula:C₂₆H₃₆O₄
Molecular Weight:412.569
Hs Code.:

Synonyms:(E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

Suppliers and Price of (E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

There total 4 articles about (E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 116103-36-7
2',6'-di-tert-butyl-4'-methylphenyl(E,2S,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-enoate

: 116103-38-9
(E)-(2R,3R,4S)-2-Benzyloxy-5-ethyl-2,4-dimethyl-hept-5-ene-1,3-diol

: 116103-37-8
(E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 9h; Heating;
DOI:10.1021/jo00255a013

Reference yield:

: 63883-81-8
3-pentanone (2,4,6-triisopropylbenzenesulfonyl)hydrazone

: 116103-37-8
(E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

Guidance literature:: Multi-step reaction with 4 steps

2: 1.) LDA / 1.) THF, -70 deg C, 30 min, 2.) 20 min

3: 97 percent / ethyl diisopropylamine / CH₂Cl₂ / 30 h / Heating

4: 72 percent / LiAlH₄ / diethyl ether / 9 h / Heating

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00255a013

Reference yield:

: 92817-95-3
(E,2S)-3-ethyl-2-methylpent-3-enal

: 116103-37-8
(E,2R,3R,4S)-2-(benzyloxy)-3-<(benzyloxy)methoxy>-5-ethyl-2,4-dimethylhept-5-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -70 deg C, 30 min, 2.) 20 min

2: 97 percent / ethyl diisopropylamine / CH₂Cl₂ / 30 h / Heating

3: 72 percent / LiAlH₄ / diethyl ether / 9 h / Heating

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00255a013