octahydro-2,4,6,8-tetramethyl-1,3,5,7-tetrakis(trimethylstannyl)-1,3,5,7,2,4,6,8-tetrazatetraborocine

Base Information

Chemical Name:octahydro-2,4,6,8-tetramethyl-1,3,5,7-tetrakis(trimethylstannyl)-1,3,5,7,2,4,6,8-tetrazatetraborocine
CAS No.:103382-76-9
Molecular Formula:C₁₆H₄₈B₄N₄Sn₄
Molecular Weight:814.668
Hs Code.:

Synonyms:octahydro-2,4,6,8-tetramethyl-1,3,5,7-tetrakis(trimethylstannyl)-1,3,5,7,2,4,6,8-tetrazatetraborocine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octahydro-2,4,6,8-tetramethyl-1,3,5,7-tetrakis(trimethylstannyl)-1,3,5,7,2,4,6,8-tetrazatetraborocine

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Technology Process of octahydro-2,4,6,8-tetramethyl-1,3,5,7-tetrakis(trimethylstannyl)-1,3,5,7,2,4,6,8-tetrazatetraborocine

There total 1 articles about octahydro-2,4,6,8-tetramethyl-1,3,5,7-tetrakis(trimethylstannyl)-1,3,5,7,2,4,6,8-tetrazatetraborocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.3%

: 17933-16-3
dibromomethylborane

: 1068-70-8
tris(trimethylstannyl)amine

: 103382-75-8
2,4-dimethyl-1,3-bis(trimethylstannyl)-1,3,2,4-diazadiboretidine

: 103382-76-9
octahydro-2,4,6,8-tetramethyl-1,3,5,7-tetrakis(trimethylstannyl)-1,3,5,7,2,4,6,8-tetrazatetraborocine

: 1066-44-0
trimethyltin bromide

Guidance literature:: In dichloromethane; under N2, N(SnMe3)3 in Ch2Cl2 added dropwise under stirring to a soln. of Sn-compound at -78°C, warmed, refluxed for 40 h; CH2Cl2 removed, Me3SnBr removed at 20°C and 5E-3 Torr, destilled at 80°C/5E-3 Torr and at 115-130°C/5E-3; elem. anal.;