methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate

Base Information

• Chemical Name: methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate
• CAS No.: 81767-34-2
• Molecular Formula: C₂₄H₃₈O₆
• Molecular Weight: 422.562
• Mol file: 81767-34-2.mol

Synonyms:methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate

Chemical Property of methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate

There total 4 articles about methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-<2-<3-hydroxy-4-(2-hydroxy-1-methylethyl)-benzoquinone-2,5>yl-2,6,6-trimethylcyclohexyl>ethanoic acid (81752-79-6) + dimethyl sulfate (77-78-1) → methyl 2-<2-(4,5-dimethoxy-3(R)-methyl-2,3-dihydrobenzofuran-6)yl-2,6,6-trimethylcyclohexyl>ethanoate (99050-64-3) + methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate (81767-34-2)

Guidance literature:

With sodium hydroxide; hydrogen; platinum(IV) oxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) methanol, 2 h, 2.) methanol, 52 h;

Reference yield:

2-<2-<3-hydroxy-4-(2-hydroxy-1-methylethyl)-benzoquinone-2,5>yl-2,6,6-trimethylcyclohexyl>ethanoic acid (81752-79-6) + dimethyl sulfate (77-78-1) → 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoic acid (99050-63-2) + {(1S,2S)-2-[2-Hydroxy-3,5-dimethoxy-4-((R)-2-methoxy-1-methyl-ethyl)-phenyl]-2,6,6-trimethyl-cyclohexyl}-acetic acid methyl ester + methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate (81767-34-2)

Guidance literature:

With sodium hydroxide; hydrogen; platinum(IV) oxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) methanol, 2 h, 2.) methanol, 11 h;

Reference yield:

{(1S,6S)-2,2,6-Trimethyl-6-[2,3,5-trihydroxy-4-((R)-2-hydroxy-1-methyl-ethyl)-phenyl]-cyclohexyl}-acetic acid + dimethyl sulfate (77-78-1) → methyl 2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoate (81767-34-2)

Guidance literature:

With sodium hydroxide; Yield given;

upstream raw materials:

2-<2-<3-hydroxy-4-(2-hydroxy-1-methylethyl)-benzoquinone-2,5>yl-2,6,6-trimethylcyclohexyl>ethanoic acid

dimethyl sulfate

Downstream raw materials:

2-<2,3,5-trimethoxy-4-(2-hydroxy-1(R)-methylethyl)-phenyl-2,6,6-trimethylcyclohexyl>ethanoic acid