(CH₂Si(CH₃)3)(C₄H₈O)Fe[C₅H₃N(C₆H₃(CH(CH₃)2)2NC(CH₃))2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(C₄₁H₆₂N₃OSi)][B(C₆H₅)4]

Base Information

• Chemical Name: (CH₂Si(CH₃)3)(C₄H₈O)Fe[C₅H₃N(C₆H₃(CH(CH₃)2)2NC(CH₃))2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(C₄₁H₆₂N₃OSi)][B(C₆H₅)4]
• CAS No.: 862169-57-1
• Molecular Formula: C₂₄H₂₀B*C₄₁H₆₂FeN₃OSi
• Molecular Weight: 1016.13

Synonyms:(CH₂Si(CH₃)3)(C₄H₈O)Fe[C₅H₃N(C₆H₃(CH(CH₃)2)2NC(CH₃))2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(C₄₁H₆₂N₃OSi)][B(C₆H₅)4]

Chemical Property of (CH₂Si(CH₃)3)(C₄H₈O)Fe[C₅H₃N(C₆H₃(CH(CH₃)2)2NC(CH₃))2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(C₄₁H₆₂N₃OSi)][B(C₆H₅)4]

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Technology Process of (CH₂Si(CH₃)3)(C₄H₈O)Fe[C₅H₃N(C₆H₃(CH(CH₃)2)2NC(CH₃))2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(C₄₁H₆₂N₃OSi)][B(C₆H₅)4]

There total 3 articles about (CH₂Si(CH₃)3)(C₄H₈O)Fe[C₅H₃N(C₆H₃(CH(CH₃)2)2NC(CH₃))2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(C₄₁H₆₂N₃OSi)][B(C₆H₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + Fe(C5H3N(CCH3NC6H3(CH(CH3)2)2)2)(CH2Si(CH3)3)(1+)*B(C6H5)4(1-)=Fe(C5H3N(CCH3NC6H3(C3H7)2)2)(SiH2C4H9)B(C6H5)4 (862169-52-6) → Fe(C5H3N(CCH3NC6H3(CH(CH3)2)2)2)(CH2Si(CH3)3)(C4H8O)(1+)*B(C6H5)4(1-)=Fe(C5H3N(NC8H6(C3H7)2)2)(SiC4H11)(C4H8O)B(C6H5)4 (862169-57-1)

Guidance literature:

In tetrahydrofuran; min THF was added to the complex; layered with pentane, -35°C for 8 h, decanted the solid was driedat room temp. under vac.; elem. anal.;

DOI:10.1021/ja106575b

Reference yield: 74.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + [Fe(CH2SiMe3)2(iPrBIP)] (862169-55-9) + N,N-dimethylanilinium tetraphenylborate → (CH2Si(CH3)3)(C4H8O)Fe[C5H3N(C6H3(CH(CH3)2)2NC(CH3))2](1+)*B(C6H5)4(1-)=[Fe(C41H62N3OSi)][B(C6H5)4] (862169-57-1)

Guidance literature:

In toluene; byproducts: C6H5N(CH3)2, Si(CH3)4;

DOI:10.1021/ja0524447

Reference yield:

((iPr)PDI)Fe(CH2SiMe3) (1005483-66-8) → Fe(C5H3N(CCH3NC6H3(CH(CH3)2)2)2)(CH2Si(CH3)3)(C4H8O)(1+)*B(C6H5)4(1-)=Fe(C5H3N(NC8H6(C3H7)2)2)(SiC4H11)(C4H8O)B(C6H5)4 (862169-57-1)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: tetrahydrofuran

In tetrahydrofuran; benzene;

DOI:10.1021/ja106575b

upstream raw materials:

tetrahydrofuran

[Fe(CH₂SiMe₃)₂(^iPrBIP)]

Fe(C₅H₃N(CCH₃NC₆H₃(CH(CH₃)2)2)2)(CH₂Si(CH₃)3)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Fe(C₅H₃N(CCH₃NC₆H₃(C₃H₇)2)2)(SiH₂C₄H₉)B(C₆H₅)4

((iPr)PDI)Fe(CH₂SiMe₃)

Downstream raw materials:

Fe(C₅H₃N(CCH₃NC₆H₃(CH(CH₃)2)2)2)(CH₂Si(CH₃)3)(C₄H₁₀O)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Fe(C₅H₃N(NC₈H₆(C₃H₇)2)2)(C₄SiH₁₁)(C₄H₁₀O)B(C₆H₅)4

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