5-Phenyl-3--cyclohexen-(2)-on

Base Information

• Chemical Name: 5-Phenyl-3--cyclohexen-(2)-on
• CAS No.: 30314-05-7
• Molecular Formula: C₂₄H₂₀O
• Molecular Weight: 324.422

Synonyms:5-Phenyl-3--cyclohexen-(2)-on

Chemical Property of 5-Phenyl-3--cyclohexen-(2)-on

Chemical Property:

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Technology Process of 5-Phenyl-3--cyclohexen-(2)-on

There total 4 articles about 5-Phenyl-3--cyclohexen-(2)-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-phenyl-cyclohexane-1,3-dione (493-72-1) → 5-Phenyl-3--cyclohexen-(2)-on (30314-05-7)

Guidance literature:

Multi-step reaction with 2 steps

1: TsOH / benzene

2: (i) Et₂O, (ii) aq. H₂SO₄

With toluene-4-sulfonic acid; In benzene;

DOI:10.1021/ja01504a051

Reference yield:

4-Biphenyl-4-yl-2-oxo-6-phenyl-cyclohex-3-enecarboxylic acid ethyl ester (30313-29-2) → 5-Phenyl-3--cyclohexen-(2)-on (30314-05-7)

Guidance literature:

With hydrogenchloride; In water; for 6h; Heating;

DOI:10.1016/j.ejmech.2005.01.005

Reference yield:

5-ethoxy-1,6-dihydro-[1,1'-biphenyl]-3(2H)-one (92251-17-7) + 4-biphenyllithium (1201-71-4) → 5-Phenyl-3--cyclohexen-(2)-on (30314-05-7)

Guidance literature:

Multistep reaction; (i) Et₂O, (ii) aq. H₂SO₄;

DOI:10.1021/ja01504a051

upstream raw materials:

5-ethoxy-1,6-dihydro-[1,1'-biphenyl]-3(2H)-one

4-biphenyllithium

4-Biphenyl-4-yl-2-oxo-6-phenyl-cyclohex-3-enecarboxylic acid ethyl ester

5-phenyl-cyclohexane-1,3-dione

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