1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol

Base Information

Chemical Name:1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol
CAS No.:1350292-76-0
Molecular Formula:C₅₅H₉₄O₆
Molecular Weight:851.348
Hs Code.:

Synonyms:1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol

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Chemical Property of 1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol

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Technology Process of 1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol

There total 14 articles about 1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1350292-75-9
1,1'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)bis-(R)-glycidol

: 100-51-6,185532-71-2
benzyl alcohol

: 1350292-76-0
1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol

Guidance literature:: With sodium methylate; at 70 ℃; for 12h; regiospecific reaction; Inert atmosphere;
DOI:10.1021/jo201827h

Reference yield: 74.0%

: 1350292-75-9
1,1'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)bis-(R)-glycidol

: 100-51-6,185532-71-2
benzyl alcohol

: 1350292-76-0
1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol

Guidance literature:: With sodium methylate; at 70 ℃; for 12h; regiospecific reaction; Inert atmosphere;
DOI:10.1021/jo201827h

Reference yield:

: 15,15'-(cis-cyclopentane-1,3-diyl)dipentadecan-1-ol

: 1350292-76-0
1,1'-di-O-benzyl-3,3'-O-((16,19-methylidene)tetratriacontane-1,34-diyl)-di-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / cyclohexane; water / 0.25 h / 20 °C

1.2: 12 h / 70 °C

2.1: sodium methylate / 12 h / 70 °C / Inert atmosphere

With tetrabutylammomium bromide; sodium methylate; sodium hydroxide; In cyclohexane; water;
DOI:10.1021/jo201827h