1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate

Base Information

Chemical Name:1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate
CAS No.:1242096-22-5
Molecular Formula:C₂₂H₃₂O₅
Molecular Weight:376.493
Hs Code.:

Synonyms:1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate

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Chemical Property of 1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate

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Technology Process of 1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate

There total 2 articles about 1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 101499-38-1
dimethyl 2,2-dimethyl-3-phenylpentane-1,5-dioate

: 158523-66-1
((1-(tert-butoxy)-2-methylprop-1-en-1-yl)oxy)trimethylsilane

: 1242096-22-5
1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 20 - 25 ℃; Inert atmosphere;
DOI:10.1039/c0cc01110j

Reference yield: 48.0%

: 31469-15-5
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

: 158523-66-1
((1-(tert-butoxy)-2-methylprop-1-en-1-yl)oxy)trimethylsilane

: 103-26-4,1754-62-7
methyl cinnamate

: 1242096-22-5
1-tert-butyl 7-methyl 2,2,6,6-tetramethyl-3-oxo-5-phenyl-1,7-heptadioate

Guidance literature:: 1-methoxy-2-methyl-1-trimethylsiloxy-1-propene; methyl cinnamate; With sodium hydroxide; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 1.5h; Inert atmosphere;

((1-(tert-butoxy)-2-methylprop-1-en-1-yl)oxy)trimethylsilane; With sodium hydroxide; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 1.5h; Inert atmosphere;

With hydrogenchloride; methanol; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 0.5h;
DOI:10.1039/c0cc01110j