C₁₃H₁₅NO₄C₃H₅NCO

Base Information

Chemical Name:C₁₃H₁₅NO₄C₃H₅NCO
CAS No.:947595-47-3
Molecular Formula:C₁₇H₂₀N₂O₅
Molecular Weight:332.356
Hs Code.:

C<sub>13</sub>H<sub>15</sub>NO<sub>4</sub>C<sub>3</sub>H<sub>5</sub>NCO

Synonyms:C₁₃H₁₅NO₄C₃H₅NCO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₅NO₄C₃H₅NCO

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Technology Process of C₁₃H₁₅NO₄C₃H₅NCO

There total 6 articles about C₁₃H₁₅NO₄C₃H₅NCO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947595-45-1
benzyl {(1S,2E)-1-[(4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]pent-2-en-1-yl}carbamate

: 947595-47-3
C₁₃H₁₅NO₄C₃H₅NCO

Guidance literature:: Multi-step reaction with 5 steps

1.1: 92 percent / Dowex 50W x8 / methanol / 26 h / Heating

2.1: 83 percent / (PCy₃)2Cl₂Ru=CHPh / benzene / 15 h / 60 °C

3.1: CSA / acetone / 6 h / 20 °C

3.2: 99 percent / H₂O; silica gel / CH₂Cl₂ / 7 h / 20 °C

4.1: CH₂Cl₂ / 0.5 h / 0 °C

5.1: 111 mg / aq. K₂CO₃ / methanol / 7 h / 20 °C

With Dowex 50W X₈; camphor-10-sulfonic acid; potassium carbonate; Grubbs catalyst first generation; In methanol; dichloromethane; acetone; benzene;
DOI:10.1021/ol0709735

Reference yield:

: 947595-38-2
benzyl {(1S,2E)-1-[(1S,2S)-1,2-dihydroxybut-3-en-1-yl]pent-2-en-1-yl}carbamate

: 947595-47-3
C₁₃H₁₅NO₄C₃H₅NCO

Guidance literature:: Multi-step reaction with 4 steps

1.1: 83 percent / (PCy₃)2Cl₂Ru=CHPh / benzene / 15 h / 60 °C

2.1: CSA / acetone / 6 h / 20 °C

2.2: 99 percent / H₂O; silica gel / CH₂Cl₂ / 7 h / 20 °C

3.1: CH₂Cl₂ / 0.5 h / 0 °C

4.1: 111 mg / aq. K₂CO₃ / methanol / 7 h / 20 °C

With camphor-10-sulfonic acid; potassium carbonate; Grubbs catalyst first generation; In methanol; dichloromethane; acetone; benzene;
DOI:10.1021/ol0709735

Reference yield:

: 33868-53-0
tributylstannyl benzyl ether

: 947595-47-3
C₁₃H₁₅NO₄C₃H₅NCO

Guidance literature:: Multi-step reaction with 6 steps

1.1: PPh₃; CBr₄; Et₃N / CH₂Cl₂ / 1.5 h / -10 °C

1.2: CH₂Cl₂ / -10 - 20 °C

1.3: 706 mg / KF / acetonitrile / 24 h / 20 °C

2.1: 92 percent / Dowex 50W x8 / methanol / 26 h / Heating

3.1: 83 percent / (PCy₃)2Cl₂Ru=CHPh / benzene / 15 h / 60 °C

4.1: CSA / acetone / 6 h / 20 °C

4.2: 99 percent / H₂O; silica gel / CH₂Cl₂ / 7 h / 20 °C

5.1: CH₂Cl₂ / 0.5 h / 0 °C

6.1: 111 mg / aq. K₂CO₃ / methanol / 7 h / 20 °C

With carbon tetrabromide; Dowex 50W X₈; camphor-10-sulfonic acid; potassium carbonate; triethylamine; triphenylphosphine; Grubbs catalyst first generation; In methanol; dichloromethane; acetone; benzene;
DOI:10.1021/ol0709735