tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate

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Chemical Name:tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate
CAS No.:1092366-06-7
Molecular Formula:C₂₇H₃₆O₅
Molecular Weight:440.58
Hs Code.:

Synonyms:tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate

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Chemical Property of tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate

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Technology Process of tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate

There total 1 articles about tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1193-47-1
2,2-dimethyl-cyclohexanone

: 1092366-05-6
(S)-methyl 1-(3-tert-butoxy-3-oxopropyl)-5-formyl-1-methyl-2,3-dihydro-1H-indene-4-carboxylate

: 1092366-06-7
tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate

Guidance literature:: 2,2-dimethyl-cyclohexanone; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

(S)-methyl 1-(3-tert-butoxy-3-oxopropyl)-5-formyl-1-methyl-2,3-dihydro-1H-indene-4-carboxylate; In tetrahydrofuran; hexane; at -78 - -30 ℃; for 2h;
DOI:10.1021/ol8024633

Reference yield: 26.0%

: 1092366-06-7
tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate

: 1092366-07-8
C₂₇H₃₈O₅

Guidance literature:: tert-butyl-3-((6S)-3-(3,3-dimethyl-2-oxocyclohexyl)-6-methyl-1-oxo-3,6,7,8-tetrahydro-1H-indeno[5,4-c]furan-6-yl)propanoate; With sodium hydroxide; In ethanol; for 0.333333h;

With palladium on carbon; hydrogen; In ethanol; for 20h; under 760.051 Torr;

With hydrogenchloride; In dichloromethane; water; pH=3;
DOI:10.1021/ol8024633