6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Base Information

Chemical Name:6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine
CAS No.:80614-88-6
Molecular Formula:C₂₀H₃₀N₂O₈
Molecular Weight:426.467
Hs Code.:

Synonyms:6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Chemical Property:

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Technology Process of 6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

There total 1 articles about 6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 80614-78-4
2',3'-O-isopropylidene-5'-O-methoxymethyl-uridine

: 80614-88-6
6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -70 deg C, 1h; 2.) THF, -70 deg C, 3.5h;
DOI:10.1016/0040-4020(82)80016-1

Reference yield: 85.3%

: 80614-88-6
6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

: 85451-59-8
6-(1-hydroxycyclohexyl)uridine

Guidance literature:: With trifluoroacetic acid; In water; for 24h; Ambient temperature;
DOI:10.1016/0040-4020(82)80016-1

Reference yield:

: 80614-88-6
6-(1-hydroxycyclohexyl)-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

: 85451-60-1
Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-(1-hydroxy-cyclohexyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85.3 percent / 50percent CF₃COOH / H₂O / 24 h / Ambient temperature

With trifluoroacetic acid; In water;
DOI:10.1016/0040-4020(82)80016-1