(Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine

Base Information

Chemical Name:(Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine
CAS No.:73557-40-1
Molecular Formula:C₁₅H₁₃Cl₂NOS₂
Molecular Weight:358.312
Hs Code.:

Synonyms:(Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine

Chemical Property:

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Technology Process of (Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine

There total 3 articles about (Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 73557-38-7
1,1-Bis(4-chlorophenylthio)-2-amino-1-propene

: 73557-40-1
(Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1021/jo01301a011

Reference yield:

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 73557-40-1
(Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine

Guidance literature:: Multi-step reaction with 3 steps

2: 68 percent / Lithium diisopropylamide / diethyl ether / 1) 0 deg C / 2h 2) 18h r.t.

3: 81 percent / m-Cl-C₆H₄-CO₃H / CH₂Cl₂ / 4 h / 0 °C

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In diethyl ether; dichloromethane;
DOI:10.1021/jo01301a011

Reference yield:

: 65276-68-8
N-<3-(4-Chlorophenylthio)-2-propylidene>benzenesulfenamide

: 73557-40-1
(Z)-2-(4-Chloro-benzenesulfinyl)-2-(4-chloro-phenylsulfanyl)-1-methyl-vinylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Lithium diisopropylamide / diethyl ether / 1) 0 deg C / 2h 2) 18h r.t.

2: 81 percent / m-Cl-C₆H₄-CO₃H / CH₂Cl₂ / 4 h / 0 °C

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In diethyl ether; dichloromethane;
DOI:10.1021/jo01301a011