4-AMIDINOBENZAMIDE HYDROCHLORIDE

Base Information

• Chemical Name: 4-AMIDINOBENZAMIDE HYDROCHLORIDE
• CAS No.: 54050-86-1
• Molecular Formula: C8H9N3O
• Molecular Weight: 199.64
• Hs Code.: 2925290090
• Mol file: 54050-86-1.mol

Synonyms:4-AMIDINOBENZAMIDE HYDROCHLORIDE;4-CARBAMIMIDOYL-BENZAMIDE,HYDROCHLORIDE;Benzamide, 4-(aminoiminomethyl)- (9CI)

Chemical Property of 4-AMIDINOBENZAMIDE HYDROCHLORIDE

Chemical Property:

• Melting Point: 302-303 °C(lit.)
• PSA: 92.96000
• LogP: 2.37190
• Solubility.: H2O: 20 mg/mL, clear, colorless

Purity/Quality:

4-Amidinobenzamide Hydrochloride 98% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-AMIDINOBENZAMIDE HYDROCHLORIDE

There total 3 articles about 4-AMIDINOBENZAMIDE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-cyanobenzamide (3034-34-2) → 4-Amidinobenzamide (54050-86-1)

Guidance literature:

With sodium amide; In dimethyl sulfoxide; Reagent/catalyst; Solvent; Sealed tube;

DOI:10.1080/00397911.2017.1330959

Reference yield:

4-aminobenzamide (2835-68-9) → 4-Amidinobenzamide (54050-86-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Diazotization

2: ethanol; benzene; hydrogen chloride / Behandeln des Reaktionsprodukts mit aethanol. Ammoniak

With hydrogenchloride; ethanol; benzene;

Reference yield:

4-cyanobenzoic Acid (619-65-8,333406-09-0) + ammonium thiocyanate (1147550-11-5) → 4-Amidinobenzamide (54050-86-1)

Guidance literature:

at 180 ℃;

DOI:10.1039/jr9470000390

upstream raw materials:

4-cyanobenzoic Acid

ammonium thiocyanate

4-cyanobenzamide

4-aminobenzamide

Downstream raw materials:

4-(aminoiminomethyl)benzoic acid hydrochloride