3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester

Base Information

Chemical Name:3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester
CAS No.:1026376-40-8
Molecular Formula:C₄₃H₃₈O₆
Molecular Weight:650.771
Hs Code.:

3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid <i>tert</i>-butyl ester

Synonyms:3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester

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Chemical Property of 3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester

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Technology Process of 3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester

There total 1 articles about 3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158980-57-5
3,5-dibenzyloxy-4-bromobenzoic acid tert-butyl ester

: 1-benzyloxy-2-naphthoyl chloride

: 1026376-40-8
3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester

Guidance literature:: 3,5-dibenzyloxy-4-bromobenzoic acid tert-butyl ester; With n-butyllithium; In tetrahydrofuran; at -68 ℃;

1-benzyloxy-2-naphthoyl chloride; In tetrahydrofuran; at -68 ℃; for 3h; Further stages.;
DOI:10.1021/jm020018f

Reference yield:

: 1026376-40-8
3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester

: 4-trans-[4-(1-hydroxy-2-naphthoyl)-3,5-dihydroxybenzoyloxy]-3-(4-hydroxybenzamido)azepane

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH

2: oxalyl chloride / CH₂Cl₂; dimethylformamide / 1 h

3: DMAP; Et₃N / CH₂Cl₂ / 0.17 h

4: H₂; TFA / Pd(OH)2 / ethanol; methanol / 2844.39 Torr

With dmap; sodium hydroxide; oxalyl dichloride; hydrogen; triethylamine; trifluoroacetic acid; palladium dihydroxide; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020018f

Reference yield:

: 1026376-40-8
3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoic acid tert-butyl ester

: 3,5-bis-benzyloxy-4-(1-benzyloxy-naphthalene-2-carbonyl)-benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH

2: oxalyl chloride / CH₂Cl₂; dimethylformamide / 1 h

With sodium hydroxide; oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020018f