(S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester

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Chemical Name:(S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester
CAS No.:76802-90-9
Molecular Formula:C₅₄H₇₇N₅O₁₃
Molecular Weight:1004.23
Hs Code.:

(S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester

Synonyms:(S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester

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Chemical Property of (S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester

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Technology Process of (S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester

There total 1 articles about (S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55878-20-1
Bpoc-Ser(Bu^t)-Thr(Bu^t)-Asp(OBu^t)-Tyr(Bu^t)-Gly-OPh

: 76802-90-9
(S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; citric acid; Yield given. Multistep reaction; 1.) acetone, H₂O, pH=10.5, 5 min; 2.) acetone, H₂O, 0 deg C, pH=4;
DOI:10.1016/0040-4020(80)80119-0

Reference yield: 66.0%

: 76802-90-9
(S)-3-{(2S,3R)-2-[(S)-2-(1-Biphenyl-4-yl-1-methyl-ethoxycarbonylamino)-3-tert-butoxy-propionylamino]-3-tert-butoxy-butyrylamino}-N-[(S)-2-(4-tert-butoxy-phenyl)-1-(carboxymethyl-carbamoyl)-ethyl]-succinamic acid tert-butyl ester

: 76803-08-2
(S)-2-[(S)-2-((2S,3S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-methyl-pentanoylamino]-4-carbamoyl-butyrylamino}-3-methyl-pentanoylamino)-3-carbamoyl-propionylamino]-3-tert-butoxy-propionic acid phenyl ester; hydrochloride

: 76803-06-0
C₉₄H₁₄₁N₁₃O₂₂

Guidance literature:: With 4-methyl-morpholine; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide; for 72h; Ambient temperature;
DOI:10.1016/0040-4020(80)80121-9