1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose

Base Information

Chemical Name:1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose
CAS No.:654075-03-3
Molecular Formula:C₂₅H₂₉O₁₀P
Molecular Weight:520.473
Hs Code.:

Synonyms:1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose

Chemical Property:

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Technology Process of 1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose

There total 2 articles about 1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 654075-02-2
2,3-di-O-benzoyl-5-bromo-5-deoxy-D-ribofuranosyl acetate

: 122-52-1
triethyl phosphite

: 654075-03-3
1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose

Guidance literature:: for 30h; Heating;
DOI:10.1021/jm00126a027

Reference yield:

: 654075-03-3
1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose

Guidance literature:

Reference yield:

: 654075-03-3
1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-(diethoxyphosphinyl)-α-D-ribofuranose

: C₂₃H₂₁N₂O₁₀P

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (NH₄)2SO₄, HMDS / 2.) TMS triflate / 1.) reflux 4 h, 2.) CH₃CN, r.t., 24 h

2: bromotrimethylsilane / acetonitrile / 6 h

With ammonium sulfate; trimethylsilyl bromide; 1,1,1,3,3,3-hexamethyl-disilazane; trimethylsilyl trifluoromethanesulfonate; In acetonitrile;
DOI:10.1021/jm00126a027