(Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:(Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline
CAS No.:154013-09-9
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

Synonyms:(Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of (Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline

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Technology Process of (Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline

There total 2 articles about (Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72258-91-4
1,2-dehydronorreticuline

: 154013-09-9
(Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 12 h / Ambient temperature

2: 28percent aq. NH₄OH

With pyridine; ammonium hydroxide; In tetrahydrofuran;
DOI:10.1021/jo00081a007

Reference yield:

: Formic acid 2-formyl-1-[1-(3-formyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-6-methoxy-1,2,3,4-tetrahydro-isoquinolin-7-yl ester

: 154013-09-9
(Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With ammonium hydroxide; Yield given;
DOI:10.1021/jo00081a007

Reference yield:

: 154013-09-9
(Z)-2-Formyl-7-hydroxy-1-<(3-hydroxy-4-methoxyphenyl)methylene>-6-methoxy-1,2,3,4-tetrahydroisoquinoline

: 72274-69-2
(+)-N-Formyl-N-norreticuline

: 72274-70-5
(-)-N-Formyl-N-norreticuline

Guidance literature:: With hydrogen; Ru<(R)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl>(OCOCH3)2; In methanol; dichloromethane; at 25 ℃; for 120h; under 38000 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00081a007