benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside

Base Information

Chemical Name:benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside
CAS No.:104875-48-1
Molecular Formula:C₂₀H₂₀FN₃O₄
Molecular Weight:385.395
Hs Code.:

Synonyms:benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside

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Technology Process of benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside

There total 7 articles about benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 104875-47-0
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

: 104875-48-1
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; at 120 ℃; for 7h;
DOI:10.1021/jo00374a013

Reference yield: 16.0%

: 81625-96-9
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-α-D-glucopyranoside

: benzyl 3-azido-2-O-benzyl-4,6-O-benzylidene-3-deoxy-D-glucopyranosyl fluoride

: 104875-48-1
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside

Guidance literature:: With diethylamino-sulfur trifluoride; In benzene; for 2h; Heating;
DOI:10.1021/jo00374a013

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 104875-48-1
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / p-toluenesulfonic acid monohydrate / dimethylformamide

2: 88 percent / pyridine / 3 h / Ambient temperature

3: 60 percent / cesium fluoride / dimethylformamide / 7 h / 120 °C

With pyridine; toluene-4-sulfonic acid; cesium fluoride; In N,N-dimethyl-formamide;
DOI:10.1021/jo00374a013