13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene

Base Information

• Chemical Name: 13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene
• CAS No.: 1224127-02-9
• Molecular Formula: C₅₀H₅₆O₆
• Molecular Weight: 752.991

Synonyms:13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene

Chemical Property of 13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene

There total 3 articles about 13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

7-oxa-8,10-dioxoundecyl 2-methyl-4-(10,10-diphenyl-9-decenyl)-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate (1224127-94-9) → 13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene (1224127-02-9)

Guidance literature:

With manganese(III) triacetate dihydrate; acetic acid; at 100 ℃; for 0.116667h; Inert atmosphere;

DOI:10.1016/j.tet.2010.02.022

Reference yield: 54.0%

hexane-1,6-diyl bis(3-oxobutanoate) (2388-18-3) + 1,1,12,12-tetraphenyl-1,11-dodecanediene (1224126-72-0) → 13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene (1224127-02-9)

Guidance literature:

With manganese(III) triacetate dihydrate; acetic acid; at 100 ℃; for 0.55h; Inert atmosphere;

DOI:10.1016/j.tet.2010.02.022

Reference yield: 14.0%

hexane-1,6-diyl bis(3-oxobutanoate) (2388-18-3) + 1,1,12,12-tetraphenyl-1,11-dodecanediene (1224126-72-0) → 13,28-dimethyl-3,10,14,27-tetraoxa-2,11-dioxo-15,15,26,26-tetraphenyltricyclo[23.3.0.0(12,16)]octacosa-12,28-diene (1224127-02-9) + 7-oxa-8,10-dioxoundecyl 2-methyl-4-(10,10-diphenyl-9-decenyl)-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate (1224127-94-9)

Guidance literature:

With manganese(III) triacetate dihydrate; acetic acid; at 100 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1016/j.tet.2010.02.022

upstream raw materials:

7-oxa-8,10-dioxoundecyl 2-methyl-4-(10,10-diphenyl-9-decenyl)-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate

hexane-1,6-diyl bis(3-oxobutanoate)

1,1,12,12-tetraphenyl-1,11-dodecanediene

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