(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-ACETIC ACID

Base Information

• Chemical Name: (5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-ACETIC ACID
• CAS No.: 53350-32-6
• Molecular Formula: C9H7ClN2O2
• Molecular Weight: 210.62
• Hs Code.: 2933990090
• Mol file: 53350-32-6.mol

Synonyms:(5-CHLORO-1H-BENZIMIDAZOL-2-YL)ACETIC ACID;(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-ACETIC ACID;CHEMBRDG-BB 4140559;ASINEX-REAG BAS 10155982;TIMTEC-BB SBB011256

Chemical Property of (5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-ACETIC ACID

Chemical Property:

• Vapor Pressure: 7.29E-12mmHg at 25°C
• Refractive Index: 1.711
• Boiling Point: 525.3°C at 760 mmHg
• Flash Point: 271.5°C
• PSA: 65.98000
• Density: 1.566g/cm³
• LogP: 1.84340
• Storage Temp.: 2-8°C

Purity/Quality:

99.3% ^*data from raw suppliers

(5-Chloro-1H-benzimidazol-2-yl)aceticAcid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-ACETIC ACID

There total 4 articles about (5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-(6-chloro-1H-benzo[d]imidazol-2-yl)acetonitrile (63928-16-5) → 6-chloro-1H-benzimidazol-2-acetic acid (53350-32-6)

Guidance literature:

With hydrogenchloride; benzenesulfonic acid; In water; for 4h; Reflux;

DOI:10.1016/j.ejmech.2016.12.014

Reference yield: 70.0%

malonic acid (141-82-2) + 4-Chloro-1,2-phenylenediamine (95-83-0) → Acide chloro-5 benzimidazolyl-2 acetique (53350-32-6)

Guidance literature:

With hydrogenchloride; for 2.5h; Heating;

Reference yield:

4-Chloro-1,2-phenylenediamine (95-83-0) + malonitrile (4341-85-9) → Acide chloro-5 benzimidazolyl-2 acetique (53350-32-6)

Guidance literature:

In sulfuric acid;

upstream raw materials:

malonic acid

4-Chloro-1,2-phenylenediamine

malonitrile

2-(6-chloro-1H-benzo[d]imidazol-2-yl)acetonitrile

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