5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Base Information

Chemical Name:5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide
CAS No.:1618132-31-2
Molecular Formula:C₄₀H₄₆ClN₄*I
Molecular Weight:745.19
Hs Code.:

5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Synonyms:5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

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Chemical Property of 5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

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Technology Process of 5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

There total 3 articles about 5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1421618-05-4
5-acetylamino-2-[2-[3-[2-(5-acetylamino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

: 1618132-31-2
5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Guidance literature:: With boron trifluoride methanol complex; In methanol; Reflux;
DOI:10.1016/j.dyepig.2014.05.002

Reference yield:

: 63857-00-1,70446-42-3
N-[(3-(anilinomethylene)-2-chloro-1-cyclohexen-1-yl)methylene]aniline hydrochloride

: 1618132-31-2
5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / ethanol

2: potassium carbonate; C₂₀H₂₉Cl₂N₅O₂Pd / water; isopropyl alcohol; chloroform / 1 h / Reflux

3: boron trifluoride methanol complex / methanol / Reflux

With C₂₀H₂₉Cl₂N₅O₂Pd; sodium acetate; boron trifluoride methanol complex; potassium carbonate; In methanol; ethanol; chloroform; water; isopropyl alcohol;
DOI:10.1016/j.dyepig.2014.05.002

Reference yield:

: 548491-82-3
C₃₈H₄₆ClN₄O₂⁽¹⁺⁾*I^(1-)

: 1618132-31-2
5-amino-2-[2-[3-[2-(5-amino-1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-chlorophenyl)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; C₂₀H₂₉Cl₂N₅O₂Pd / water; isopropyl alcohol; chloroform / 1 h / Reflux

2: boron trifluoride methanol complex / methanol / Reflux

With C₂₀H₂₉Cl₂N₅O₂Pd; boron trifluoride methanol complex; potassium carbonate; In methanol; chloroform; water; isopropyl alcohol;
DOI:10.1016/j.dyepig.2014.05.002