Technology Process of C16H15N3O2S
There total 6 articles about C16H15N3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon;
In
toluene;
at 100 ℃;
for 24h;
Sealed tube;
DOI:10.2174/1570178611310040002
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 20 h / 100 °C
2: triethylsilane; trifluoroacetic acid / dichloromethane / 0 - 20 °C
3: palladium 10% on activated carbon / toluene / 24 h / 100 °C / Sealed tube
With
triethylsilane; palladium 10% on activated carbon; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid;
In
dichloromethane; toluene;
1: |Buchwald-Hartwig Coupling;
DOI:10.2174/1570178611310040002
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylsilane; trifluoroacetic acid / dichloromethane / 0 - 20 °C
2: palladium 10% on activated carbon / toluene / 24 h / 100 °C / Sealed tube
With
triethylsilane; palladium 10% on activated carbon; trifluoroacetic acid;
In
dichloromethane; toluene;
DOI:10.2174/1570178611310040002