(2-((tert-butoxycarbonyl)oxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate

Base Information

Chemical Name:(2-((tert-butoxycarbonyl)oxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate
CAS No.:1383708-43-7
Molecular Formula:C₁₉H₂₆O₇Zn
Molecular Weight:431.801
Hs Code.:

Synonyms:(2-((tert-butoxycarbonyl)oxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate

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Chemical Property of (2-((tert-butoxycarbonyl)oxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate

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Technology Process of (2-((tert-butoxycarbonyl)oxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate

There total 4 articles about (2-((tert-butoxycarbonyl)oxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 918402-86-5
3-tert-butoxycarbonyloxy-benzoic acid ethyl ester

: zinc trimethylacetate

: 1383708-43-7
(2-((tert-butoxycarbonyl)oxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate

Guidance literature:: 3-tert-butoxycarbonyloxy-benzoic acid ethyl ester; With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere; Schlenk technique;

zinc trimethylacetate; In tetrahydrofuran; at 0 - 25 ℃; for 0.25h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201403015

Reference yield:

: 918402-86-5
3-tert-butoxycarbonyloxy-benzoic acid ethyl ester

: zinc trimethylacetate

: 1383708-43-7
(2-(tert-butoxycarbonyloxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate

Guidance literature:: 3-tert-butoxycarbonyloxy-benzoic acid ethyl ester; With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere; Schlenk technique;

zinc trimethylacetate; In tetrahydrofuran; at 0 - 25 ℃; for 0.25h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201204526

Reference yield:

: 815-17-8
trimethylpyruvic acid

: 1383708-43-7
(2-(tert-butoxycarbonyloxy)-6-(ethoxycarbonyl)phenyl)zinc pivalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylzinc / tetrahydrofuran / 1.5 h / 0 - 25 °C / Inert atmosphere

2.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere; Schlenk technique

2.2: 0.25 h / 0 - 25 °C / Inert atmosphere; Schlenk technique

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; diethylzinc; In tetrahydrofuran;
DOI:10.1002/anie.201204526