CH₂C(CH₃)CHNBn

Base Information

• Chemical Name: CH₂C(CH₃)CHNBn
• CAS No.: 27760-62-9
• Molecular Formula: C₁₁H₁₃N
• Molecular Weight: 159.231
• Mol file: 27760-62-9.mol

Synonyms:CH₂C(CH₃)CHNBn

Chemical Property of CH₂C(CH₃)CHNBn

Chemical Property:

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Technology Process of CH₂C(CH₃)CHNBn

There total 1 articles about CH₂C(CH₃)CHNBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylpropenal (78-85-3,25120-30-3) + benzylamine (100-46-9) → CH2C(CH3)CHNBn (27760-62-9)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 1.5h; Molecular sieve;

DOI:10.1039/c2cc36129a

Reference yield: 12.0%

n-octyne (629-05-0) + CH2C(CH3)CHNBn (27760-62-9) → N-benzyl-2-heptyl-4-methylpyrrole (1201072-97-0)

Guidance literature:

With chlorobis(cyclooctene)rhodium(I) dimer; tricyclohexylphosphine; In toluene; at 110 ℃; for 9h; Inert atmosphere;

DOI:10.1002/anie.200904402

Reference yield:

CH2C(CH3)CHNBn (27760-62-9) + 1-(trimethylsilyl)-3-phenylprop-1-yne (31683-47-3) → C23H29NSi (1016970-56-1)

Guidance literature:

With chlorobis(cyclooctene)rhodium(I) dimer; diethyl-{4-dimethylamino-phenyl}-phosphine; In toluene; at 100 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja312311k

upstream raw materials:

2-methylpropenal

benzylamine

Downstream raw materials:

N-benzyl-2-heptyl-4-methylpyrrole

C₂₃H₂₉NSi

C₂₀H₂₃N