(4,5-Diiodo-1,2-phenylene)dimethanol

Base Information

Chemical Name:(4,5-Diiodo-1,2-phenylene)dimethanol
CAS No.:53279-73-5
Molecular Formula:C8H8I2O2
Molecular Weight:389.959
Hs Code.:2906299090
DSSTox Substance ID:DTXSID30478930
Wikidata:Q82312660
Mol file:53279-73-5.mol

Synonyms:53279-73-5;(4,5-Diiodo-1,2-phenylene)dimethanol;CELERYKETONE;DTXSID30478930;AKOS015964752

Suppliers and Price of (4,5-Diiodo-1,2-phenylene)dimethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(4,5-Diiodo-1,2-phenylene)dimethanol 95+%
1g
$ 581.00

Chemenu
(4,5-diiodo-1,2-phenylene)dimethanol 95%
1g
$ 549.00

American Custom Chemicals Corporation
(2-HYDROXYMETHYL-4,5-DIIODO-PHENYL)-METHANOL 95.00%
5MG
$ 501.97

Alichem
(4,5-Diiodo-1,2-phenylene)dimethanol
1g
$ 511.92

Total 3 raw suppliers

Chemical Property of (4,5-Diiodo-1,2-phenylene)dimethanol

Chemical Property:

Vapor Pressure:4.73E-07mmHg at 25°C
Refractive Index:1.739
Boiling Point:398.1°C at 760 mmHg
Flash Point:194.6°C
PSA：40.46000
Density:2.418g/cm³
LogP:1.88040
Storage Temp.:2-8°C
XLogP3:1.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:389.86137
Heavy Atom Count:12
Complexity:127

Purity/Quality:

≥99% ^*data from raw suppliers

(4,5-Diiodo-1,2-phenylene)dimethanol 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=CC(=C1I)I)CO)CO

Technology Process of (4,5-Diiodo-1,2-phenylene)dimethanol

There total 4 articles about (4,5-Diiodo-1,2-phenylene)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 82679-28-5
4,5-diiodobenzene-1,2-dicarboxylic acid

: 53279-73-5
4,5-diiodobenzene-1,2-dicarbinol

Guidance literature:: 4,5-diiodobenzene-1,2-dicarboxylic acid; With borane-THF; In tetrahydrofuran; at 0 - 66 ℃; for 42h; Inert atmosphere;

With potassium carbonate; In tetrahydrofuran; water; at 50 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2016.06.064

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 53279-73-5
4,5-diiodobenzene-1,2-dicarbinol

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; fuming sulfuric acid / 40 h / 85 °C

2.1: potassium hydroxide / water / 20 h / 100 °C

3.1: borane-THF / tetrahydrofuran / 42 h / 0 - 66 °C / Inert atmosphere

3.2: 12 h / 50 °C / Inert atmosphere

With borane-THF; fuming sulfuric acid; iodine; potassium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2016.06.064

Reference yield:

: 68218-30-4
4,5-diiodophthalimide

: 53279-73-5
4,5-diiodobenzene-1,2-dicarbinol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / water / 20 h / 100 °C

2.1: borane-THF / tetrahydrofuran / 42 h / 0 - 66 °C / Inert atmosphere

2.2: 12 h / 50 °C / Inert atmosphere

With borane-THF; potassium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2016.06.064