C₄₄H₆₁NO₉Si

Base Information

Chemical Name:C₄₄H₆₁NO₉Si
CAS No.:1446749-26-3
Molecular Formula:C₄₄H₆₁NO₉Si
Molecular Weight:776.055
Hs Code.:

C<sub>44</sub>H<sub>61</sub>NO<sub>9</sub>Si

Synonyms:C₄₄H₆₁NO₉Si

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Chemical Property of C₄₄H₆₁NO₉Si

Chemical Property:

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Technology Process of C₄₄H₆₁NO₉Si

There total 9 articles about C₄₄H₆₁NO₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1446749-05-8
C₂₇H₄₅N₃O₁₁Si

: 1446749-26-3
C₄₄H₆₁NO₉Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C

1.2: IR-120 resin

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

2.2: 2 h / 0 - 20 °C

3.1: triphenylphosphine / tetrahydrofuran; water / 12 h / 20 °C

4.1: pyridine / 12 h / 0 - 20 °C

With pyridine; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204550

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 1446749-26-3
C₄₄H₆₁NO₉Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Molecular sieve

2.1: trifluoroacetic acid; trifluoroacetic anhydride / dichloromethane / 0.5 h / 0 °C

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Molecular sieve; Inert atmosphere

4.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C

4.2: IR-120 resin

5.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

5.2: 2 h / 0 - 20 °C

6.1: triphenylphosphine / tetrahydrofuran; water / 12 h / 20 °C

7.1: pyridine / 12 h / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204550

Reference yield:

: 941280-63-3
(2R,3S,4R)-2-hydroxy-3,4-O-isopropylidene-1-trityloxy-hex-5-ene

: 1446749-26-3
C₄₄H₆₁NO₉Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Molecular sieve

2.1: trifluoroacetic acid; trifluoroacetic anhydride / dichloromethane / 0.5 h / 0 °C

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Molecular sieve; Inert atmosphere

4.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C

4.2: IR-120 resin

5.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

5.2: 2 h / 0 - 20 °C

6.1: triphenylphosphine / tetrahydrofuran; water / 12 h / 20 °C

7.1: pyridine / 12 h / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204550