ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate

Base Information

Chemical Name:ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate
CAS No.:173365-15-6
Molecular Formula:C₂₉H₂₉NO₅
Molecular Weight:471.553
Hs Code.:

Synonyms:ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate

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Chemical Property of ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate

Chemical Property:

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Technology Process of ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate

There total 1 articles about ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-81-4
4-Methylbenzyl bromide

: 152360-09-3
Ethyl 4-[3-(3,4-dihydroxybenzoyl)indol-1-yl]butanoate

: 173365-15-6
ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0960-894X(99)00230-9

Reference yield:

: 173365-15-6
ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate

: 4-{3-[3-{3-[4-(2-isopropoxy-phenyl)-piperazin-1-yl]-propoxy}-4-(4-methyl-benzyloxy)-benzoyl]-indol-1-yl}-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature

2: KI, K₂CO₃ / dimethylformamide / 60 °C

3: aq. KOH / methanol / Heating

With potassium hydroxide; potassium carbonate; potassium iodide; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(99)00230-9

Reference yield:

: 173365-15-6
ethyl 4-{3-[3-hydroxy-4-(4-methylphenylmethoxy)benzoyl]indol-1-yl}butanoate

: 4-{3-[3-{3-[4-(2-ethoxy-phenyl)-piperazin-1-yl]-propoxy}-4-(4-methyl-benzyloxy)-benzoyl]-indol-1-yl}-butyric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature

2: KI, K₂CO₃ / dimethylformamide / 60 °C

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(99)00230-9