tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate

Base Information

Chemical Name:tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate
CAS No.:1203706-72-2
Molecular Formula:C₁₉H₂₈N₂O₅
Molecular Weight:364.442
Hs Code.:

Synonyms:tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate

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Chemical Property of tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate

Chemical Property:

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Technology Process of tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate

There total 2 articles about tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2044-64-6
N,N-Dimethylacetoacetamid

: 479423-40-0
N-tert-butyl 4-methoxybenzylidenecarbamate

: 1203706-72-2
tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate

: tert-butyl 2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate

Guidance literature:: With n-butyllithium; (R)-3,3′-bis(3,4,5-trifluorophenyl)[1,1′-binaphthalene]-2,2′-diol; tert-butyl alcohol; In hexane; toluene; at -78 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja909874b

Reference yield:

: 2044-64-6
N,N-Dimethylacetoacetamid

: 479423-40-0
N-tert-butyl 4-methoxybenzylidenecarbamate

: 1203706-72-2
tert-butyl (1R,2S)-2-(dimethylcarbamoyl)-1-(4-methoxyphenyl)-3-oxobutylcarbamate

: C₁₉H₂₈N₂O₅

Guidance literature:: With n-butyllithium; (R)-3,3′-bis(3,4,5-trifluorophenyl)[1,1′-binaphthalene]-2,2′-diol; tert-butyl alcohol; In hexane; toluene; at -78 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0030-1258296